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Download e-book for kindle: ASM Handbook: Materials Characterization by George M. Crankovic

By George M. Crankovic

ISBN-10: 0871700166

ISBN-13: 9780871700162

Will give you an simply understood reference booklet on glossy analytical suggestions. It emphasizes the sensible particularly the theoretical, describing the commonest purposes and barriers of every process.

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Extra info for ASM Handbook: Materials Characterization

Example text

Such samples are often crushed to obtain small particle sizes that promote improved mixing. Crushers can range from the familiar mortar and pestle to specially designed mills. They must be made of noncontaminating materials harder than the materials processed to minimize abrasion and should have chemical resistivity to the samples. The fineness of grinding required will depend on the heterogeneity of the sample, but fine grinding is ordinarily preferred. Sieving may be performed at intermediate stages to separate fines and coarses that are later reground.

If an entrance slit is located on a circle of radius R/2 tangent to the grating face, the diffracted images of the slit are focused around the circle. Exit slits and photomultiplier tubes may be placed at positions on the focal curve corresponding to wavelengths of lines from various elements. Line intensities from 40 to more than 60 elements, depending on instrument capability, can be determined simultaneously. Fig. 6 Light path through a Rowland circle grating mount. Alternatively, a strip of film or a photographic plate may be positioned in the focal curve in place of the slits and photomultiplier tubes, converting the polychromator into a spectrograph.

Taylor, Quality Assurance of Chemical Measurements, Anal. , Vol 53, 1981, p 1588A-1595A 15. A. M. J. , John Wiley & Sons, 1979, p 299-359 16. R. Moody, NBS Clean Laboratories for Trace Elemental Analysis, Anal. , Vol 54, 1982, p 1358A1376A 17. "Standard Practice for Preparation of Sediment Samples for Chemical Analysis," D 3976, Annual Book of ASTM Standards, ASTM, Philadelphia, 1984, p 673-676 18. R. K. H. Harrison, Chemical Homogenization of Biological Tissues, Anal. , Vol 55, 1983, p 2431 19.

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ASM Handbook: Materials Characterization by George M. Crankovic


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